Nanostructured Coatings of 3d-Metals Produced by Green Chemistry Methods: Analysis of Inhomogeneities by Static and Dynamic Magnetic Methods

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Abstract

The study investigates carbon-containing coatings of 3d-metals (Ni, Co, Fe) produced by chemical deposition method using arabinogalactan. The coatings were analyzed using X-ray diffraction, FMR, and M(H) magnetometry. Measurement of M(H) in plane and perpendicular to the plane of the magnetic coatings allowed determining the distribution of demagnetizing factor in the studied coatings. The obtained distributions of the demagnetizing factor were used to analyze the angular dependences of the ferromagnetic resonance field. The values of magnetization and perpendicular anisotropy field were estimated. The paper illustrates the effect of texture on the magnetic parameters.

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About the authors

I. G. Vazhenina

Kirensky Institute of Physics – a branch of the Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences; Siberian Federal University

Author for correspondence.
Email: irina-vazhenina@mail.ru
Russian Federation, Krasnoyarsk; Krasnoyarsk

S. V. Stolyar

Siberian Federal University; Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences

Email: irina-vazhenina@mail.ru
Russian Federation, Krasnoyarsk; Krasnoyarsk

S. V. Komogortsev

Kirensky Institute of Physics – a branch of the Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences; Reshetnev Siberian State University of Science and Technology

Email: irina-vazhenina@mail.ru
Russian Federation, Krasnoyarsk; Krasnoyarsk

O. A. Li

Siberian Federal University; Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences

Email: irina-vazhenina@mail.ru
Russian Federation, Krasnoyarsk; Krasnoyarsk

R. S. Iskhakov

Kirensky Institute of Physics – a branch of the Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences

Email: irina-vazhenina@mail.ru
Russian Federation, Krasnoyarsk

D. A. Velikanov

Kirensky Institute of Physics – a branch of the Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences

Email: irina-vazhenina@mail.ru
Russian Federation, Krasnoyarsk

E. V. Cheremiskina

Siberian Federal University

Email: irina-vazhenina@mail.ru
Russian Federation, Krasnoyarsk

I. V. Nemtsev

Kirensky Institute of Physics – a branch of the Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences; Siberian Federal University; Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences

Email: irina-vazhenina@mail.ru
Russian Federation, Krasnoyarsk; Krasnoyarsk; Krasnoyarsk

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Supplementary files

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2. Fig. 1. X-ray diffraction data of Fe/C (a), Ni/C (b), Co/C (c) coatings and element cards from the ICDD database under each diffractogram. Each peak has the value of the interplanar distance in Å in front of the chemical element symbol, with Miller indices in brackets

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3. Fig. 2. SEM images of Fe/C (a) and Ni-C (b) coatings. The inset of the Fe/C SEM image shows the X-ray surface mapping

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4. Fig. 3. Schematic illustrating the geometry of the experiment

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5. Fig. 4. Approximation of magnetisation to saturation using iron coating as an example. The black solid line is the fitting by equation (1)

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6. Fig. 5. Magnetisation curves (a, b, c) in the field directed parallel (H||) and perpendicular (H⊥) to the plane of Fe (a), Co (b) and Ni (c) carbon-containing coatings, as well as histograms of the effective internal field distribution (d, e, f)

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7. Fig. 6. Angular dependences of the resonance fields of coatings based on Fe/C (a, d), Co/C (b, e) and Ni/C (c, f) alloys and examples of spectra at φH = 0°

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8. Fig. 7. Angular dependences of the resonance field of Fe/C (a), Co/C (b) and Ni/C (c) coatings. The rhombuses indicate the experimental values, the solid line shows the fitting curve calculated by taking into account the inhomogeneous internal field, the dashed line shows the fitting curve in the case of a homogeneous thin film. The insets show experimental FMR curves at some angles between the normal (z-axis) and the external field direction, as well as curves used in the decomposition of the experimental spectrum

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