Magnetic Properties of a Nickel–Zinc Ferrite Powder with Different Degrees of Dispersion

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The influence of the degree of dispersion of a nickel–zinc ferrite powder of a Ni0.7Zn0.3Fe2O4 composition on its magnetic properties has been considered. The material has been synthesized using the ceramic technology with preliminary mechanical activation of precursors. The degree of dispersion has been varied using different modes of its dry grinding in a ball mill. The patterns of the changes in saturation magnetization and the coercive force as a function of grinding modes and a specific surface area of the ferrite powder have been established. The changes in the pattern of the magnetic phase transition in the region of the Curie temperature of materials with different degrees of dispersion have been determined.

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作者简介

S. Bobuyok

National Research Tomsk Polytechnic University

编辑信件的主要联系方式.
Email: sab45@tpu.ru
俄罗斯联邦, Tomsk

A. Surzhikov

National Research Tomsk Polytechnic University

Email: sab45@tpu.ru
俄罗斯联邦, Tomsk

E. Lysenko

National Research Tomsk Polytechnic University

Email: sab45@tpu.ru
俄罗斯联邦, Tomsk

E. Nikolaev

National Research Tomsk Polytechnic University

Email: sab45@tpu.ru
俄罗斯联邦, Tomsk

V. Salnikov

Immanuel Kant Baltic Federal University

Email: sab45@tpu.ru
俄罗斯联邦, Kaliningrad

参考

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2. Fig. 1. Experimental cell for TMM [7]

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3. Fig. 2. Thermal anomaly parameters on TG/DTG curves obtained during TMM of magnetic samples: Tnach/Tcon - transition start/end temperature; ΔT - transition temperature range; Δm - transition weight step; TC - Curie temperature

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4. Fig. 3. X-ray diffraction pattern of synthesised NCF (▼ - position of reflexes of Ni0.73Zn0.29Fe1.98O4 phase)

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5. Fig. 4. Results of BET analysis: Sud - specific surface area, m2/g

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6. Fig. 5. Particle size distributions of NCF powders based on volume (Q3)

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7. Fig. 6. Hysteresis loops of NCF samples with different specific surface area

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8. Fig. 7. Dependence of saturation magnetisation on NCF grinding modes

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9. Fig. 8. Dependence of coercive force on NCF grinding modes

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10. Fig. 9. Thermograms of samples in the Curie temperature region

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11. Fig. 10. Dependence of the parameter Δm of the thermal anomaly at the Curie point on the specific surface area Sud of NCF powder

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